Laboratory Medicine ›› 2017, Vol. 32 ›› Issue (7): 642-646.DOI: 10.3969/j.issn.1673-8640.2017.07.020
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PAN Xilong, LIU Xiaodong, HUANG Shaofen
Received:
2016-06-06
Online:
2017-08-08
Published:
2017-08-09
CLC Number:
PAN Xilong, LIU Xiaodong, HUANG Shaofen. Measurement uncertainties for the determinations of serum K+,Na+ and Cl- and their quality improvement[J]. Laboratory Medicine, 2017, 32(7): 642-646.
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URL: https://www.shjyyx.com/EN/10.3969/j.issn.1673-8640.2017.07.020
分析 项目 | 质控品 批号 | 质控品水平(mmol/L) | 日间CV(%) | 日间CV均值 (%) |
---|---|---|---|---|
K+A1 | 172688 | 3.65 | 2.23 | 2.17 |
K+A2 | 174794 | 3.77 | 2.10 | |
K+B1 | 170153 | 6.42 | 1.92 | 1.99 |
K+B2 | 174801 | 6.52 | 2.06 | |
Na+A1 | 172688 | 112.00 | 1.55 | 1.63 |
Na+A2 | 174794 | 113.00 | 1.70 | |
Na+B1 | 170153 | 136.00 | 1.63 | 1.57 |
Na+B2 | 174801 | 139.00 | 1.51 | |
Cl-A1 | 172688 | 76.80 | 2.94 | 2.76 |
Cl-A2 | 174794 | 75.30 | 2.58 | |
Cl-B1 | 170153 | 105.20 | 2.36 | 2.46 |
Cl-B2 | 174801 | 106.80 | 2.55 |
分析 项目 | 质控品 批号 | 质控品水平(mmol/L) | 日间CV(%) | 日间CV均值 (%) |
---|---|---|---|---|
K+A1 | 172688 | 3.65 | 2.23 | 2.17 |
K+A2 | 174794 | 3.77 | 2.10 | |
K+B1 | 170153 | 6.42 | 1.92 | 1.99 |
K+B2 | 174801 | 6.52 | 2.06 | |
Na+A1 | 172688 | 112.00 | 1.55 | 1.63 |
Na+A2 | 174794 | 113.00 | 1.70 | |
Na+B1 | 170153 | 136.00 | 1.63 | 1.57 |
Na+B2 | 174801 | 139.00 | 1.51 | |
Cl-A1 | 172688 | 76.80 | 2.94 | 2.76 |
Cl-A2 | 174794 | 75.30 | 2.58 | |
Cl-B1 | 170153 | 105.20 | 2.36 | 2.46 |
Cl-B2 | 174801 | 106.80 | 2.55 |
分析 项目 | 批号 | 实验室数 | 实验室均值(mmol/L) | 本室测定值(mmol/L) | CV (%) |
---|---|---|---|---|---|
K+a1 | 201311 | 706 | 4.07 | 4.11 | 2.78 |
K+a2 | 201325 | 694 | 4.11 | 4.28 | 5.69 |
K+a3 | 201331 | 687 | 4.06 | 4.00 | 2.37 |
K+a4 | 201414 | 724 | 4.08 | 4.18 | 3.00 |
K+a5 | 201421 | 719 | 3.85 | 3.87 | 3.00 |
K+a6 | 201433 | 721 | 4.41 | 4.66 | 2.65 |
K+a7 | 201515 | 751 | 3.67 | 3.81 | 6.05 |
K+a8 | 201524 | 742 | 3.77 | 4.07 | 2.92 |
K+a9 | 201531 | 735 | 3.64 | 3.73 | 3.18 |
K+a10 | 201613 | 771 | 4.12 | 4.22 | 2.72 |
Na+a1 | 201314 | 58 | 107.00 | 108.00 | 1.86 |
Na+a2 | 201323 | 61 | 121.00 | 123.00 | 1.29 |
Na+a3 | 201332 | 59 | 106.00 | 104.00 | 1.51 |
Na+a4 | 201415 | 70 | 108.00 | 108.00 | 2.35 |
Na+a5 | 201423 | 71 | 111.00 | 108.00 | 2.32 |
Na+a6 | 201434 | 69 | 111.00 | 114.00 | 2.16 |
Na+a7 | 201512 | 74 | 114.00 | 112.00 | 4.78 |
Na+a8 | 201523 | 78 | 107.00 | 111.00 | 2.39 |
Na+a9 | 201534 | 74 | 111.00 | 112.00 | 1.45 |
Na+a10 | 201615 | 78 | 122.00 | 123.00 | 1.34 |
Cl-a1 | 201312 | 56 | 77.90 | 76.90 | 3.12 |
Cl-a2 | 201323 | 59 | 78.30 | 79.80 | 3.15 |
Cl-a3 | 201332 | 57 | 74.80 | 75.60 | 2.85 |
Cl-a4 | 201415 | 67 | 73.30 | 72.80 | 3.19 |
Cl-a5 | 201423 | 68 | 73.30 | 69.70 | 2.98 |
Cl-a6 | 201434 | 65 | 72.40 | 71.40 | 3.05 |
Cl-a7 | 201512 | 72 | 71.80 | 73.50 | 4.85 |
Cl-a8 | 201523 | 73 | 68.90 | 70.50 | 3.80 |
Cl-a9 | 201534 | 70 | 72.50 | 72.20 | 2.37 |
Cl-a10 | 201615 | 77 | 74.60 | 72.50 | 1.99 |
K+b1 | 201314 | 701 | 6.90 | 7.19 | 4.00 |
K+b2 | 201324 | 695 | 6.83 | 7.20 | 5.40 |
K+b3 | 201332 | 682 | 6.87 | 6.92 | 2.78 |
K+b4 | 201332 | 716 | 6.76 | 6.79 | 4.01 |
K+b5 | 201411 | 719 | 6.66 | 6.52 | 3.84 |
K+b6 | 201422 | 718 | 7.00 | 7.22 | 3.39 |
K+b7 | 201432 | 743 | 5.70 | 5.87 | 3.21 |
K+b8 | 201514 | 753 | 6.89 | 7.29 | 6.22 |
K+b9 | 201525 | 731 | 6.72 | 6.88 | 3.38 |
K+b10 | 201614 | 775 | 6.32 | 6.40 | 3.32 |
Na+b1 | 201315 | 58 | 136.00 | 136.00 | 1.18 |
Na+b2 | 201325 | 60 | 152.00 | 155.00 | 1.37 |
Na+b3 | 201334 | 58 | 130.00 | 128.00 | 1.37 |
Na+b4 | 201412 | 70 | 135.00 | 135.00 | 1.73 |
Na+b5 | 201425 | 71 | 141.00 | 137.00 | 1.93 |
Na+b6 | 201431 | 70 | 132.00 | 135.00 | 1.80 |
Na+b7 | 201513 | 75 | 139.00 | 137.00 | 2.90 |
Na+b8 | 201522 | 78 | 138.00 | 141.00 | 1.52 |
Na+b9 | 201535 | 74 | 142.00 | 143.00 | 1.72 |
Na+b10 | 201611 | 80 | 141.00 | 142.00 | 1.65 |
Cl-b1 | 201313 | 57 | 107.70 | 110.60 | 2.51 |
Cl-b2 | 201322 | 58 | 107.20 | 111.60 | 2.21 |
Cl-b3 | 201335 | 58 | 107.90 | 108.10 | 2.01 |
Cl-b4 | 201413 | 68 | 103.60 | 101.40 | 2.20 |
Cl-b5 | 201424 | 66 | 103.90 | 103.80 | 2.23 |
Cl-b6 | 201435 | 66 | 102.60 | 105.60 | 2.81 |
Cl-b7 | 201511 | 71 | 105.40 | 107.00 | 2.50 |
Cl-b8 | 201521 | 76 | 107.30 | 111.50 | 2.18 |
Cl-b9 | 201535 | 71 | 96.40 | 96.00 | 1.85 |
Cl-b10 | 201614 | 77 | 103.90 | 105.20 | 2.08 |
分析 项目 | 批号 | 实验室数 | 实验室均值(mmol/L) | 本室测定值(mmol/L) | CV (%) |
---|---|---|---|---|---|
K+a1 | 201311 | 706 | 4.07 | 4.11 | 2.78 |
K+a2 | 201325 | 694 | 4.11 | 4.28 | 5.69 |
K+a3 | 201331 | 687 | 4.06 | 4.00 | 2.37 |
K+a4 | 201414 | 724 | 4.08 | 4.18 | 3.00 |
K+a5 | 201421 | 719 | 3.85 | 3.87 | 3.00 |
K+a6 | 201433 | 721 | 4.41 | 4.66 | 2.65 |
K+a7 | 201515 | 751 | 3.67 | 3.81 | 6.05 |
K+a8 | 201524 | 742 | 3.77 | 4.07 | 2.92 |
K+a9 | 201531 | 735 | 3.64 | 3.73 | 3.18 |
K+a10 | 201613 | 771 | 4.12 | 4.22 | 2.72 |
Na+a1 | 201314 | 58 | 107.00 | 108.00 | 1.86 |
Na+a2 | 201323 | 61 | 121.00 | 123.00 | 1.29 |
Na+a3 | 201332 | 59 | 106.00 | 104.00 | 1.51 |
Na+a4 | 201415 | 70 | 108.00 | 108.00 | 2.35 |
Na+a5 | 201423 | 71 | 111.00 | 108.00 | 2.32 |
Na+a6 | 201434 | 69 | 111.00 | 114.00 | 2.16 |
Na+a7 | 201512 | 74 | 114.00 | 112.00 | 4.78 |
Na+a8 | 201523 | 78 | 107.00 | 111.00 | 2.39 |
Na+a9 | 201534 | 74 | 111.00 | 112.00 | 1.45 |
Na+a10 | 201615 | 78 | 122.00 | 123.00 | 1.34 |
Cl-a1 | 201312 | 56 | 77.90 | 76.90 | 3.12 |
Cl-a2 | 201323 | 59 | 78.30 | 79.80 | 3.15 |
Cl-a3 | 201332 | 57 | 74.80 | 75.60 | 2.85 |
Cl-a4 | 201415 | 67 | 73.30 | 72.80 | 3.19 |
Cl-a5 | 201423 | 68 | 73.30 | 69.70 | 2.98 |
Cl-a6 | 201434 | 65 | 72.40 | 71.40 | 3.05 |
Cl-a7 | 201512 | 72 | 71.80 | 73.50 | 4.85 |
Cl-a8 | 201523 | 73 | 68.90 | 70.50 | 3.80 |
Cl-a9 | 201534 | 70 | 72.50 | 72.20 | 2.37 |
Cl-a10 | 201615 | 77 | 74.60 | 72.50 | 1.99 |
K+b1 | 201314 | 701 | 6.90 | 7.19 | 4.00 |
K+b2 | 201324 | 695 | 6.83 | 7.20 | 5.40 |
K+b3 | 201332 | 682 | 6.87 | 6.92 | 2.78 |
K+b4 | 201332 | 716 | 6.76 | 6.79 | 4.01 |
K+b5 | 201411 | 719 | 6.66 | 6.52 | 3.84 |
K+b6 | 201422 | 718 | 7.00 | 7.22 | 3.39 |
K+b7 | 201432 | 743 | 5.70 | 5.87 | 3.21 |
K+b8 | 201514 | 753 | 6.89 | 7.29 | 6.22 |
K+b9 | 201525 | 731 | 6.72 | 6.88 | 3.38 |
K+b10 | 201614 | 775 | 6.32 | 6.40 | 3.32 |
Na+b1 | 201315 | 58 | 136.00 | 136.00 | 1.18 |
Na+b2 | 201325 | 60 | 152.00 | 155.00 | 1.37 |
Na+b3 | 201334 | 58 | 130.00 | 128.00 | 1.37 |
Na+b4 | 201412 | 70 | 135.00 | 135.00 | 1.73 |
Na+b5 | 201425 | 71 | 141.00 | 137.00 | 1.93 |
Na+b6 | 201431 | 70 | 132.00 | 135.00 | 1.80 |
Na+b7 | 201513 | 75 | 139.00 | 137.00 | 2.90 |
Na+b8 | 201522 | 78 | 138.00 | 141.00 | 1.52 |
Na+b9 | 201535 | 74 | 142.00 | 143.00 | 1.72 |
Na+b10 | 201611 | 80 | 141.00 | 142.00 | 1.65 |
Cl-b1 | 201313 | 57 | 107.70 | 110.60 | 2.51 |
Cl-b2 | 201322 | 58 | 107.20 | 111.60 | 2.21 |
Cl-b3 | 201335 | 58 | 107.90 | 108.10 | 2.01 |
Cl-b4 | 201413 | 68 | 103.60 | 101.40 | 2.20 |
Cl-b5 | 201424 | 66 | 103.90 | 103.80 | 2.23 |
Cl-b6 | 201435 | 66 | 102.60 | 105.60 | 2.81 |
Cl-b7 | 201511 | 71 | 105.40 | 107.00 | 2.50 |
Cl-b8 | 201521 | 76 | 107.30 | 111.50 | 2.18 |
Cl-b9 | 201535 | 71 | 96.40 | 96.00 | 1.85 |
Cl-b10 | 201614 | 77 | 103.90 | 105.20 | 2.08 |
分析项目 | 浓度范围 (mmol/L) | Urel(Rw) (%) | RMSrel(bias) (%) | Urel(Cref) (%) | Ucrel(bias) (%) | Ucrel (%) | Urel (%) |
---|---|---|---|---|---|---|---|
K+A | 3.64~4.41 | 2.17 | 3.85 | 0.13 | 3.86 | 4.42 | 8.84 |
K+B | 5.70~7.00 | 1.99 | 3.33 | 0.14 | 3.33 | 3.88 | 7.76 |
Na+A | 106~122 | 1.63 | 2.01 | 0.26 | 2.02 | 2.60 | 5.20 |
Na+B | 130~152 | 1.57 | 1.65 | 0.32 | 1.68 | 2.30 | 4.60 |
Cl-A | 68.9~78.3 | 2.76 | 2.24 | 0.39 | 2.27 | 3.57 | 7.15 |
Cl-B | 96.4~107.9 | 2.46 | 2.37 | 0.27 | 2.39 | 3.43 | 6.86 |
分析项目 | 浓度范围 (mmol/L) | Urel(Rw) (%) | RMSrel(bias) (%) | Urel(Cref) (%) | Ucrel(bias) (%) | Ucrel (%) | Urel (%) |
---|---|---|---|---|---|---|---|
K+A | 3.64~4.41 | 2.17 | 3.85 | 0.13 | 3.86 | 4.42 | 8.84 |
K+B | 5.70~7.00 | 1.99 | 3.33 | 0.14 | 3.33 | 3.88 | 7.76 |
Na+A | 106~122 | 1.63 | 2.01 | 0.26 | 2.02 | 2.60 | 5.20 |
Na+B | 130~152 | 1.57 | 1.65 | 0.32 | 1.68 | 2.30 | 4.60 |
Cl-A | 68.9~78.3 | 2.76 | 2.24 | 0.39 | 2.27 | 3.57 | 7.15 |
Cl-B | 96.4~107.9 | 2.46 | 2.37 | 0.27 | 2.39 | 3.43 | 6.86 |
分析项目 | Urel(Rw) | Ucrel(bias) | 改进重点 | |||||
---|---|---|---|---|---|---|---|---|
目标值 | 实测值 | 是否达标 | 目标值 | 实测值 | 是否达标 | |||
K+ | 2.5 | 2.17 | 是 | 2.0 | 3.86 | 否 | 正确度 | |
1.99 | 是 | 3.33 | 否 | 正确度 | ||||
Na+ | 1.5 | 1.63 | 否 | 1.5 | 2.02 | 否 | 精密度和正确度 | |
1.57 | 否 | 1.68 | 否 | 精密度和正确度 | ||||
Cl- | 1.5 | 2.76 | 否 | 1.5 | 2.27 | 否 | 精密度和正确度 | |
2.46 | 否 | 2.39 | 否 | 精密度和正确度 |
分析项目 | Urel(Rw) | Ucrel(bias) | 改进重点 | |||||
---|---|---|---|---|---|---|---|---|
目标值 | 实测值 | 是否达标 | 目标值 | 实测值 | 是否达标 | |||
K+ | 2.5 | 2.17 | 是 | 2.0 | 3.86 | 否 | 正确度 | |
1.99 | 是 | 3.33 | 否 | 正确度 | ||||
Na+ | 1.5 | 1.63 | 否 | 1.5 | 2.02 | 否 | 精密度和正确度 | |
1.57 | 否 | 1.68 | 否 | 精密度和正确度 | ||||
Cl- | 1.5 | 2.76 | 否 | 1.5 | 2.27 | 否 | 精密度和正确度 | |
2.46 | 否 | 2.39 | 否 | 精密度和正确度 |
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